Title: Effect of tomography resolution on calculation of microstructural properties for lithium ion porous electrodes
Authors: Le Houx, James
Osenberg, Markus
Neumann, Matthias
Binder, Joachim R.
Schmidt, Volker
Manke, Ingo
Carraro, Thomas  
Kramer, Denis 
Language: en
Subject (DDC): DDC::500 Naturwissenschaften und Mathematik::540 Chemie::541 Physikalische Chemie
Issue Date: 2020
Publisher: Electrochemical Society
Document Type: Article
Journal / Series / Working Paper (HSU): ECS transactions : ECST 
Volume: 97
Issue: 7
Page Start: 255
Page End: 266
Publisher Place: Pennington, NJ
Abstract: 
This work uses an open-source, data-driven, image-based modelling framework; OpenImpala. Lithium Iron Phosphate (LFP) electrode samples were imaged using micro-CT. Two scans were performed using the Zeiss 160 kVp Versa 510 at the University of Southampton. The two scans were both carried out on the same sample and using the same focal point, this is so they could be used as a direct comparison to see how porosity and tortuosity changed with spatial resolution. It is found that the Bruggeman correlation significantly underestimates the tortuosity compared to the OpenImpala calculated results. It is also found that there is a larger statistical variability in the 801 nm results, whereas the 400 nm results have a much smaller standard deviation. These results were compared to computer-generated images based on FIB/SEM tomographic data of a single Nickel Manganese Cobalt Oxide (NMC) porous active particle and found to have the same trends.
Organization Units (connected with the publication): Computational Material Design 
URL: https://iopscience.iop.org/article/10.1149/09707.0255ecst
ISSN: 1938-5862
DOI: 10.1149/09707.0255ecst
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